Investigation of Bi2O3-rich part of Bi2O3–PbO phase diagram

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Published: Dec 30, 2017
DOI: https://doi.org/10.2298/JSC170711111D
Keywords:
Bi2O3 PbO phase diagram

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Aleksandra Dapčević
University of Belgrade, Department of General and Inorganic Chemistry, Faculty of Technology and Metallurgy, Karnegijeva 4, 11000 Belgrade
Dejan Poleti
University of Belgrade, Department of General and Inorganic Chemistry, Faculty of Technology and Metallurgy, Karnegijeva 4, 11000 Belgrade
Ljiljana Karanović
University of Belgrade, Laboratory of Crystallography, Faculty of Mining and Geology, Đušina 7, 11000 Belgrade
Jelena Miladinović
University of Belgrade, Department of Inorganic Chemical Technology, Faculty of Technology and Metallurgy, Karnegijeva 4, 11000 Belgrade

Abstract

A new Bi-rich part of Bi2O3 - PbO phase diagram was determined using differential thermal analysis and X-ray powder diffraction techniques. Four solid solutions, α‑Bi2O3, γ‑Bi2O3, δ-Bi2O3 and βss-Bi8Pb5O17, can be distinguished below 37.5 mol% of PbO and one compound, β2-Bi8Pb5O17. Two of them, δ-Bi2O3 and βss-Bi8Pb5O17 are high-temperature phases. The large field of γ‑Bi2O3 stability was implemented making the crucial difference comparing to phase diagrams from the Bi2O3 - PbO system published so far.

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How to Cite
[1]
A. Dapčević, D. Poleti, L. Karanović, and J. Miladinović, “Investigation of Bi2O3-rich part of Bi2O3–PbO phase diagram”, J. Serb. Chem. Soc., vol. 82, no. 12, pp. 1433–1444, Dec. 2017.
Issue
Vol. 82 No. 12 (2017)
Section
Materials

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