Signal amplification for sumatriptan sensing based on polymeric surface decorated with Cu nanoparticles

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Published: Apr 30, 2018
DOI: https://doi.org/10.2298/JSC170727006K
Keywords:
sumatriptan melamine glassy carbon electrode copper nanoparticles differential pulse voltammetry.

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Ghasem Karim-Nezhad
Department of Chemistry, Payame Noor University, P.O. BOX 19395-3697 Tehran
Samane Khanaliloo
Department of Chemistry, Payame Noor University, P.O. BOX 19395-3697 Tehran
Zeynab Khorablou
Department of Chemistry, Payame Noor University, P.O. BOX 19395-3697 Tehran
Parisa Seyed Dorraji
Department of Chemistry, Payame Noor University, P.O. BOX 19395-3697 Tehran

Abstract

A new nanocomposite (Cu NPs/poly melamine) was deposited on glassy carbon electrode by cyclic voltammetry. Uniform deposition of the nanocomposite was observed by field emission scanning electron microscopy. The electron transfer characteristics of sumatriptan (SUM), was greatly improved on the modified electrode. The prepared electrode was used for sensitive determination of SUM by differential pulse voltammetry. Linear calibration curve was obtained in the concentration ranges of 0.08 - 0.58 and 0.58 – 6.5 μM, and detection limit of 0.025 µM. The proposed method was evaluated by determination of SUM in human biological fluids such as urine and blood plasma with satisfactory results (recovery > 99 %).

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How to Cite
[1]
G. Karim-Nezhad, S. Khanaliloo, Z. Khorablou, and P. Seyed Dorraji, “Signal amplification for sumatriptan sensing based on polymeric surface decorated with Cu nanoparticles”, J. Serb. Chem. Soc., vol. 83, no. 4, pp. 449–462, Apr. 2018.
Issue
Vol. 83 No. 4 (2018)
Section
Electrochemistry

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