Thermal, morphological and surface properties of composite materials with perlite reinforcement
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Abstract
This paper deals with the preparation and characterization of perlite/polyvinyl alcohol, perlite/polyvinylpyrrolidone, perlite/polymethyl methacrylate, and perlite/polystyrene composites. Polymer composites were prepared by solvent casting technique with 5 wt. % of perlite filler. Perlite is a filler with unique properties, such as low density and thermal conductivity, thus the development of Polymer-Perlite composites may be interesting for producing lighter packaging with thermal insulation capability. The perlite/polymer nanocomposites were characterized using X-ray diffraction (XRD) analysis, thermogravimetric analysis (TGA), Fourier-transform infrared spectroscopy (FTIR), inverse gas chromatography (IGC), field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM). TGA measurements showed remarkable increases in the thermal stability of the polystyrene by the perlite loading as compared to the matrix. The FE-SEM image of the cryomilled sample shows that the perlite particles were embedded within a polystyrene matrix. This finding is consistent with the work of adhesion data obtained by IGC.
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