Signal amplification for sumatriptan sensing based on polymeric surface decorated with Cu nanoparticles

Authors

  • Ghasem Karim-Nezhad Department of Chemistry, Payame Noor University, P.O. BOX 19395-3697 Tehran
  • Samane Khanaliloo Department of Chemistry, Payame Noor University, P.O. BOX 19395-3697 Tehran
  • Zeynab Khorablou Department of Chemistry, Payame Noor University, P.O. BOX 19395-3697 Tehran
  • Parisa Seyed Dorraji Department of Chemistry, Payame Noor University, P.O. BOX 19395-3697 Tehran

DOI:

https://doi.org/10.2298/JSC170727006K

Keywords:

sumatriptan, melamine, glassy carbon electrode, copper nanoparticles, differential pulse voltammetry.

Abstract

A new nanocomposite (Cu NPs/poly melamine) was deposited on glassy carbon electrode by cyclic voltammetry. Uniform deposition of the nanocomposite was observed by field emission scanning electron microscopy. The electron transfer characteristics of sumatriptan (SUM), was greatly improved on the modified electrode. The prepared electrode was used for sensitive determination of SUM by differential pulse voltammetry. Linear calibration curve was obtained in the concentration ranges of 0.08 - 0.58 and 0.58 6.5 μM, and detection limit of 0.025 µM. The proposed method was evaluated by determination of SUM in human biological fluids such as urine and blood plasma with satisfactory results (recovery > 99 %).

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Published

2018-04-30

How to Cite

[1]
G. Karim-Nezhad, S. Khanaliloo, Z. Khorablou, and P. Seyed Dorraji, “Signal amplification for sumatriptan sensing based on polymeric surface decorated with Cu nanoparticles”, J. Serb. Chem. Soc., vol. 83, no. 4, pp. 449-462, Apr. 2018.

Issue

Section

Electrochemistry