Screen printed carbon electrode modified with magnetic core shell manganese ferrite nanoparticles for electrochemical detection of amlodipine

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Published: Oct 6, 2019
DOI: https://doi.org/10.2298/JSC1810056036M
Keywords:
amlodipine determination magnetic core shell nanoparticles screen-printed carbon electrode

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Sayed Zia Mohammadi
Department of Chemistry, Payame Noor University, Tehran
Somayeh Tajik
Research Center of Tropical and Infectious Diseases, Kerman University of Medical Sciences, Kerman
Hadi Beitollahi
Environment Department, Institute of Science and High Technology and Environmental Sciences, Graduate University of Advanced Technology, Kerman

Abstract

In the present work, a rapid and sensitive detection of the amlodipine (AML) based on the modified screen printed carbon electrode (SPCE) is dev­eloped. At first, SPCE was modified with magnetic core shell manganese fer­rite nanoparticles (MCSNP). Cyclic voltammetry (CV) was used to study the electrochemical behaviour of AML and its determination was conducted by applying differential pulse voltammetry (DPV). The results were showed that, the modified SPCE in comparison with unmodified SPCE exhibited the enhanced electrocatalytic activity toward the oxidation of AML. A single irreversible oxidation peak was observed at a potentials of 600 and 725 mV (on the scale of Ag/AgCl electrode) on the modified SPCE and unmodified SPCE, respectively. Under the optimized conditions, the anodic peak current of AML recorded by DPV varies linearly with AML concentration in the range 0.5–400 µM with a detection limit of 0.1 µM. The modified SPCE was used for the quantitative analysis of AML in AML tablet and urine samples and the results indicated the feasibility of the developed method for AML analysis in routine detection.

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How to Cite
[1]
S. Z. Mohammadi, S. Tajik, and H. Beitollahi, “Screen printed carbon electrode modified with magnetic core shell manganese ferrite nanoparticles for electrochemical detection of amlodipine”, J. Serb. Chem. Soc., vol. 84, no. 9, pp. 1005–1016, Oct. 2019.
Issue
Vol. 84 No. 9 (2019)
Section
Electrochemistry

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Author Biography

Sayed Zia Mohammadi, Department of Chemistry, Payame Noor University, Tehran

Department of Chemistry, Payame Noor University, Tehran, Iran
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